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		<Ref>AAN6842B10012</Ref>
		<FAuthor>Ruiz-Jimenez J. , Luque de Castro M. D.* </FAuthor>
		<ArtTitle>Coupling microdialysis to capillary electrophoresis.</ArtTitle>
		<CommonTitle>TrAC Trends in Analytical Chemistry</CommonTitle>
		<TitleCitedAs>Trends Anal. Chem.</TitleCitedAs>
		<SubYear>2006</SubYear>
		<Volume>25</Volume>
		<Issue>6</Issue>
		<FPage>563</FPage>
		<LPage>571</LPage>
		<Abstract>An overview of the most outstanding aspects of microdialysis (MD) and capillary electrophoresis (CE) separately, but especially the promising trend of their off and on-line coupling is presented here. The interfaces required and the main advantages of MD-CE arrangements as compared with those used in MD-HPLC are emphasized as well as key applications of MD-CE in pharmacokinetics, pharmacodynamics and neuroscience. (62 references).</Abstract>
	</Record>
	<Record>
		<Ref>AAN6842C10013</Ref>
		<FAuthor>Matusiewicz H. , Krawczyk M. </FAuthor>
		<ArtTitle>Determination of cadmium and lead in reference materials by volatile species generation with in situ trapping flame atomic absorption spectrometry.</ArtTitle>
		<CommonTitle>Microchemical Journal</CommonTitle>
		<TitleCitedAs>Microchem. J.</TitleCitedAs>
		<SubYear>2006</SubYear>
		<Volume>83</Volume>
		<Issue>1</Issue>
		<FPage>17</FPage>
		<LPage>23</LPage>
		<Abstract>The analytical performance of coupled volatile species generation-integrated atom trap (VSG-IAT) atomizer flame atomic absorption spectrometry (FAAS) system was evaluated for determination of Cd and Pb in reference materials. Lead using formation of PbH
			<inf>4</inf> and Cd
			<sup>0</sup> vapors are atomized in air-acetylene flame-heated IAT. A new design of VSG-IAT-FAAS hyphenated technique that would exceed the operational capabilities of existing arrangements (a water-cooled single silica tube, double-slotted quartz tube or an &ldquo;integrated trap&rdquo;) was investigated. A dramatic improvement in detection limit was achieved compared with that obtained using either of the above atom trapping techniques separately. The concentration detection limits, defined as 3 times the blank standard deviation (3&sigma;), were 0.05 and 0.40 ng mL
			<sup>&minus;1</sup> for Cd and Pb, respectively. For a 120 s in situ pre-concentration time, sensitivity enhancement compared to flame AAS, was 500 and 575 folds for Cd and Pb, respectively, using volatile species generator-atom trapping technique. The sensitivity can be further improved by increasing the collection time. The precision, expressed as RSD, was 4.4% and 4.1% (
			<it>n</it> = 6) for Cd and Pb, respectively. The designs studied include slotted tube, single silica tube and integrated atom trap-cooled atom traps. The accuracy of method was verified using certified reference materials (PLANTS 3 and IAEA/W-4) by standard additional calibration technique. The measured Cd and Pb contents in two reference materials were in satisfactory agreement with the certified values.
		</Abstract>
		<XLink>http://dx.doi.org/10.1080/00032710801935095</XLink>
	</Record>
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