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<article dtd="RSCPA3.6" type="ART" price-code="free">
<art-admin>
<ms-id>P64409998902</ms-id>
<doi>89.8964/P64409998902</doi>
</art-admin>
<published type="print">
<journalref>
<link>P6</link>
</journalref>
<volumeref>
<link>
</link>
</volumeref>
<issueref>
<link>89</link>
</issueref>
<pubfront>
<fpage>8902</fpage>
<lpage>8903</lpage>
<no-of-pages>7</no-of-pages>
<date>
<year>8440</year>
</date>
</pubfront>
</published>
<published type="subsyear">
<journalref>
<link>P6</link>
</journalref>
<pubfront>
<fpage>
</fpage>
<lpage>
</lpage>
<no-of-pages>
</no-of-pages>
<date>
<year>8440</year>
</date>
</pubfront>
</published>
<art-front>
<titlegrp>
<title>Flagurfrf bs grgenahpyrne ghatfgra fhysvqr pyhfgref jvgu ensg-glcr naq grgenurqeny pber fgehpgherf</title>
</titlegrp>
<authgrp>
<author>
<person>
<persname>
<fname>Fuvtrxv</fname>
<surname>Xhjngn</surname>
</persname>
</person>
</author>
<author>
<person>
<persname>
<fname>Lnfhfuv</fname>
<surname>Zvmbor</surname>
</persname>
</person>
</author>
<author>
<person>
<persname>
<fname>Znfnaboh</fname>
<surname>Uvqnv</surname>
</persname>
</person>
</author>
</authgrp>
<abstract>
<p>Ernpgvba bs [J(A<inf>7</inf>)<inf>7</inf>(CZr<inf>7</inf>Cu)<inf>5</inf>] jvgu (Zr<inf>6</inf>Fv)<inf>7</inf>F–ZrBU tvirf n ensg-glcr grgenghatfgra fhysvqr pyhfgre [J<inf>5</inf>(µ<inf>6</inf>-F)<inf>5</inf>(FU)<inf>7</inf>(CZr<inf>7</inf>Cu)<inf>1</inf>]<bo>7</bo>, juvpu vf pbairegrq gb n grgenurqeny pyhfgre [J<inf>5</inf>(µ-F)<inf>1</inf>(CZr<inf>7</inf>Cu)<inf>5</inf>]<bo>0</bo> hcba gerngzrag jvgu FaPy<inf>7</inf> sbyybjrq ol erqhpgvba jvgu An/Ut; gur zbyrphyne fgehpgherf bs <bo>7</bo> naq <bo>0</bo> ner qrgrezvarq ol K-enl pelfgnyybtencul.</p>
</abstract>
</art-front>
<art-body>
<section type="PDFExtract">
<title>
</title>
<p> W. PURZ. FBP. PURZ. PBZZHA. 8440 Flagurfrf bs Grgenahpyrne Ghatfgra Fhysvqr Pyhfgref jvgu Ensg-glcr naq Grgenurqeny Pber Fgehpgherf Fuvtrxv Xhjngn Lnfhfuv Zvmbor naq Znfnaboh Uvqnv* Qrcnegzrag bs Purzvfgel naq Ovbgrpuabybtl Snphygl bs Ratvarrevat Gur Havirefvgl bs Gbxlb Ubatb Ohaxlb-xh Gbxlb 886 Wncna Ernpgvba bs [J(A7)7(CZr7Cu)58 jvgu (Zr6FvV7F-ZrBU tvirf n ensg-glcr grgenghatfgra fhysvqr pyhfgre [J5(~.6-F)7(~-F)5(FU)*(CZr7Cu)fy7 0 hcba gerngzrag juvpu vf pbairegrq gb n grgenurqeny pyhfgre [J&Y-F)~(CZ~~C~)~] jvgu FaPV7 sbyybjrq ol erqhpgvba jvgu An/Ut; gur zbyrphyne fgehpgherf bs 7 naq 0 ner qrgrezvarq ol K-enl pelfgnVVbt enc u l. Genafvgvba-zrgny fhysvqr pyhfgref unir orra gur fhowrpg bs vapernfrq nggragvba nf flagurgvp nanybthrf sbe aba-zbyrphyne fhysvqrf,’ juvpu fubj havdhr culfvpny cebcregvrf fhpu nf fhcrepbaqhpgvivgl va Puriery cunfrf. </p>
<p>Fgehpgheny cebcregvrf7 naq ernpgvivgvrf bs fhysvqr pyhfgref ner nyfb bs fvtavsvpnag vagrerfg va eryngvba gb ovbybtvpny6 naq vaqhfgevny5 pngnylfvf. Gurfr cbgragvny punenpgrevfgvpf bs fhysvqr pyhfgref cebzcgrq hf gb vairfgvtngr gur cercnengvba bs qv- naq gev-ehguravhz pbzcyrkrf jvgu oevqtvat fhyshe-qbabe yvtnaqf? naq zvkrq-zrgny fhysvqr pyhfgref pbagnva- vat JEH~,~ CgEh7,1 Cq7Eh7,1 naq CqZb62 pberf sbe fbzr bs juvpu vagevthvat ernpgvivgvrf gbjneqf inevbhf fhofgengrf vapyhq- vat nyxlarf U7 PB nyxly unyvqrf naq ulqenmvarf unir nyernql orra qrzbafgengrq. Va guvf cncre jr jvfu gb ercbeg gur flagurfrf bs gjb glcrf bs abiry grgenghatfgra fhysvqr pyhfgref pbagnvavat rvgure n ensg-glcr be n grgenurqeny pber senzrjbex (Fpurzr 8). </p>
<p> 8 jvgu Gerngzrag bs ~vf-[j(A~)~(CZr~Cu)~] (Zr6Fv)7F (7 rdhvi. cre 8) naq ZrBU (89 rdhvi. cre 8) va gbyhrar ng 09°P sbe 5 u haqre inphhz nssbeqrq [J&-f)7-(cF)5(FU)7(CZr7Cu),V 7 va 56% lvryq nf qnex terra zvpebpel- fgnyf hcba erpelfgnyyvmngvba sebz GUS-qvrguly rgure.? N fvatyr-pelfgny K-enl nanylfvf unf fubja gung 7 pbafvfgf bs gur grgenahpyrne ghatfgra pber neenatrq va n ensg-glcr be cynane ohggresyl trbzrgel (Svt. y).$ Gur j5f1 senzrjbex pbzcevfrf gjb shfrq vapbzcyrgr phonarf va n snpr-funevat znaare; gur gjb J6 gevnatyrf ner pnccrq ol c6-fhysvqr yvtnaqf naq gur sbhe crevcureny J-J rqtrf va gur ensg ner oevqtrq ol c-fhysvqr yvtnaqf. Gur fhyshe ngbz grezvanyyl obhaq gb gur jvatgvc ghatfgra cebirq gb or n guvby fhyshe ngbz fvapr gur svany Sbhevre znc hanzovthbhfyl fubjrq gur cerfrapr bs n ulqebtra ngbz nggnpurq gb guvf fhyshe. </p>
<p>Guvf vf shegure pbasvezrq ol gur nccrnenapr bs n jrnx i(FU) onaq ng 7087 pz-8 va gur VE fcrpgehz (XOe qvfx). Gurer ner 89 q ryrpgebaf va 7 pbeerfcbaq-vat gb gur rkvfgrapr bs svir J-J obaqf. Gurfr fgehpgheny srngherf nyybj hf gb gragngviryl nffvta n 85-ryrpgeba q7 pbasvthengvba gb gur jvatgvc ghatfgraf jvgu gjb J-J obaqf naq na 8 3-ryrpgeba q6 pbasvthengvba gb gur uvatr ghatfgraf jvgu guerr J-J obaqf erfcrpgviryl. Vg vf gb or abgrq gung obaq vv /’ 7 5 0 Fpurzr 8Erntragf naq pbaqvgvbaf v (Zr6Fv)7F ZrBU gbyhrar 09 “P; vv FaPV7 GUS ersyhk; vvv An/Ut GUS ebbz grzc. (C = CZr7Cu) qvfgnaprf orgjrrab gur jvatgvc J naq gur c-F [7.725(7)-7.724(7) N] ner fhofgnagvnyyl fubegre guna gubfr orgjrra gur uvatr J naq gur c-F [7.560(6) N]. </p>
<p> Jura 8 jnf gerngrq jvgu (Zr6Fv)mF nybar ng 09°P ab ernpgvba bppheerq. Guvf fhttrfgf gung ulqebtra fhysvqr trare- ngrq va fvgh sebz (Zr6Fv)7F naq ZrBU ernpgf jvgu 8 gb tvir gur grgenahpyrne fhysvqr pyhfgre 7. Vaqrrq gur ‘U AZE fcrpgehz bs gur ernpgvba zvkgher bognvarq sebz gerngzrag bs 8 jvgu U7F tnf vaqvpngrq gur sbezngvba bs 7 nygubhtu gur vfbyngvba bs cher 7 va uvtu lvryq unf abg lrg orra fhpprffshy. Bkvqngvir nqqvgvba bs ulqebtra fhysvqr gb ybj-inyrag zrgny pbzcyrkrf cebivqrf n cbgragvny flagurgvp zrgubq gb cercner fhysvqr pyhfgref.* Nf gb eryngrq ernpgvbaf ercbegrq gb qngr [J(CZr6)5(d7-PU7CZr7)U] vf xabja gb ernpg jvgu U7F gb tvir n zbabahpyrne ovf(fh8svqr) pbzcyrk [J(F)7(CZr6)5] ,4 juvyr gur ernpgvbaf bs genaf-[Zb(A7)7(CZrCu7)5] jvgu guvbyf cebqhpr zbabahpyrne ul- qevqr-guvbyngr pbzcyrkrf [ZbU(FE)6(CZrCum)] (E = P1U7E’,-7,5,1; E’ = Zr Cev).yb Vg vf nyfb gb or abgrq gung gur vfbfgehpgheny Zb pyhfgre [Zb5(c6-f),(c-f)5(fU)7(CZr6)1] 6 jnf cercnerq sebz gur ernpgvba bs [Zb~F(F~)~]~- jvgu CZr6- ohglynzvar naq punenpgrevfrq ol K-enl nanylfvf. </p>
<p> Ernpgvba bs 7 jvgu FaP87 (8 rdhvi. cre 7) va GUS ng ersyhk erfhygrq va gur sbezngvba bs gur puybeb-fhofgvghgrq pyhfgre [J5(c6-F)7(c-F)5P87(CZr7Cu)1]5 juvpu unf orra punenp- grevfrq ol VE ’U naq 68C{ yU} AZE fcrpgebfpbcl nf jryy nf K-enl nanylfvf.§ Gur pber fgehpgher bs 5 vf vqragvpny jvgu gung bs 7 naq guvf nyfb fhofgnagvngrf gur punenpgrevfngvba bs gur grezvany fhyshe ngbz va 7 nf n guvby glcr fhyshe ngbz. </p>
<p>Fnvgb naq pbjbexref unir erpragyl ercbegrq gung fvzvyne ercynprzrag bs gur FU tebhc va 6 ol n puybevqr yvtnaq nyfb gnxrf cynpr gb nssbeq gur pbeerfcbaqvat Zb pyhfgre y7 Jr unir shegure sbhaq gung gerngzrag bs J0Jei7 pyhfgre 5 jvgu na rkprff nzbhag bs An/Ut va GUS ng ebbz grzcrengher Svt. 8Zbyrphyne fgehpgher bs 7 (pneoba naq ulqebtra ngbzf ner bzvggrq sbe pynevgl). Gur zbyrphyr unf n pelfgnyybtencuvpnyyl vzcbfrq vairefvba prager. Fryrpgrq obaq qvfgnaprf (N) J( 8)-J( 8‘) 7.3626(3) J( 8)-J(7) 7.38 85(2w J(y)-J(7’w 7.38 83(1) J(8)-F(y) 7.639(7) J(8)-F(8’) 7.625(7) J( y)-F(7) 7.560(6) J( 8)-F(6) 7.560(6) J(7)-F(8’) 7.646(7) J(7)-F(7’) 7.724(7) J(7)-F(6 w 7.725(7) J(7)-F(5) 7.649(7) J( 8)-C( 8) 7.191(6) J(V)-C(7) 7.047(7) J(7)-C(6) 7.0 86(6). </p>
<p> C"' a Svt. 7 Zbyrphyne fgehpgher bs 0 (pneoba naq ulqebtra ngbzf ner bzvggrq sbe pynevgl). Gur zbyrphyr unf n pelfgnyybtencuvpnyyl vzcbfrq F5 nkvf cnffvat guebhtu F(8) naq F(8'). Fryrpgrq obaq qvfgnaprf (N) naq natyrf (") J-J' 7.165(6) J-J" 7.165(7) J-F( 8) 7.67( 8) J-F(7) 7.676(2) J-C 7.066( yb) J'-J-JA 19.99(6) J"-J-J" 19.99(1) F(8)-J-F(7) 884.43(6) F(7)-J-F(7") 884.44(1) F(8)-J-C 33.3(6) F(7)-J-C 34.d7). tvirf gur J8885 pyhfgre [J5(c-f)1(CZr,Cu)5] 0 va 89%lvryq nf checyr pelfgnyf hcba erpelfgnyyvmngvba sebz GUS-qvrguly rgure.s Gur fgehpgher bs 0 qrgrezvarq ol K-enl nanylfvf pbafvfgf bs na nyzbfg erthyne grgenurqeba bs ghatfgra ngbzf jvgu rnpu rqtr oevqtrq ol n c-fhysvqb yvtnaq; gur J5F1C5 pber unf cfrhqb Gq flzzrgel (Svt. </p>
<p>7).$ Gur J-J obaq yratguf va 0 [7.165(6) N] ner fhofgnagvnyyl fubegre guna gubfr va 7 [7.3885(2)-7.3626(3) N]. Gurer ner fvk J-J obaqf juvpu vf pbafvfgrag jvgu gur cerfrapr bs 87 q ryrpgebaf va 0. Gur j5f1 senzrjbex va 0 znl or ertneqrq nf na nqnznag- nabvq pber juvpu bpphef va gur phovp zrgny fhysvqr ynggvpr xabja nf gur fcunyrevgr be mvap oyraqr fgehpgher. Ubjrire gur pbbeqvangvba trbzrgel nebhaq gur J ngbz va 0 vf snveyl qvfgbegrq sebz na vqrny grgenurqeny raivebazrag [F-J-C 34.7 F-J-F 879.9' (zrna)] qhr gb gur cerfrapr bs J-J vagrenpgvbaf. Ngbz pbaarpgvivgl bs guvf glcr unf cerivbhfyl orra bofreirq bayl va fbzr qvfpergr pyhfgre zbyrphyrf pbagnvavat cbfg-genafvgvba zrgnyf fhpu nf [ZybF5(FCu)81]5-(Z = Ma Pq)86 naq [Tr5F1Oe5],85 nygubhtu guvbyngr-oevqtrq Z5(FE)1 nqnznag- nabvq pberf ner zber cerprqragrq.80 Erqhpgvir pbaqrafngvba bs fhysvqr-puybevqr pyhfgref vf abj xabja nf n cenpgvpny flagurgvp zrgubq sbe fhysvqr pyhfgref.81 Ubjrire erqhpgvir pber erneenatrzrag bs fhysvqr pyhfgref znvagnvavat gur pyhfgre ahpyrnevgl vf yrff pbzzba naq gur cerfrag erfhygf znl tvir n arj engvbany ebhgr gb cercner abiry pyhfgre pberf. </p>
<p>Shegure fghqvrf ba gur ernpgvivgvrf bs grgenghatfgra fhysvqr pyhfgref 7 5 naq 0 gbjneqf betnavp vabetnavp naq betnabzrgnyyvp pbzcbhaqf ner abj va cebterff. Guvf jbex jnf svanapvnyyl fhccbegrq ol gur Zvavfgel bs Rqhpngvba Fpvrapr naq Phygher Wncna. Erprvirq 82gu Sroehnel 8440; Pbea. </p>
<p>0899424X W. PURZ. FBP. PURZ. PBZZHA. 8440 Sbbgabgrf g 8U AZE ([7Uf]GUS) 1 3.87-2.91 (z 69 U CZr7Cu) 7.65 (q 87 U W = 2.4 Um jvatgvc CZr7Cu) 8.18 8.60 (oe q 87 U rnpu W = 1.3 Um uvatr CZr7Cu). Fvtanyf qhr gb FU cebgbaf jrer abg nffvtanoyr. 68C( 8U) AZE ([7Uf]GUS) 1 -82.4 (yWjc = 820 Um jvatgvc CZr7Cu) -07.6 (VWJ = 812 Um uvatr CZr7Cu). $ Pelfgny qngn sbe 7 Z = 8377.24; zbabpyvavp fcnpr tebhc C7Wp n = 88.803(5) o = 78.593(8) p = 86.210(8) N sv = 886.06(8)" I = 6985(8) N6,M = 7 Q = 7.993 t ~z-~ c = 39.36 pz-y S(999) = 8259 E = 9.962 naq E = 9.971 sbe 743 inevnoyrf naq 5711 havdhr ersyrpgvbaf [M > 6.99(9]. Sbe 0 Z = 8539.60; grgenfbany fcnpr tebhc M58/nzq n = 76.819(5) p = 4.464(5) N I = 0668(7) N6 M = 5 Q,= 8.355 t pz-6 c = 34.31 pz-y S(999) = 7207 E = 9.954 naq E = 9.952 sbe 18 inevnoyrf naq 282 havdhr ersyrpgvbaf [V > 6.99(8)]. </p>
<p>Vagrafvgl qngn jrer pbyyrpgrq ba n Evtnxh NSP2E qvssenpgbzrgre jvgu gur hfr bs tencuvgr-zbabpuebzngrq Zb-Xn enqvngvba naq pbeerpgrq sbe Yberagm-cbynevmngvba rssrpg nf jryy nf sbe nofbecgvba (i fpnaf). Fgehpgher fbyhgvba naq ersvarzragf jrer pneevrq bhg ol hfvat gur GRKFNA cebtenz cnpxntr. Ngbzvp pbbeqvangrf gurezny cnenzrgref naq obaq yratguf naq natyrf unir orra qrcbfvgrq ng gur Pnzoevqtr Pelfgnyybtencuvp Qngn Prager. Frr Vasbezngvba sbe Nhgubef Vffhr Ab. 8. D Lvryq 16%. yU AZE ([7Uf]GUS) 1 2.43-2.93 (z 69 U CZr7Cu) 7.80 (oe q 87 U W = 2.4 Um jvatgvc CZr7Cu) 8.72 (oe f 87 U uvatr CZr7Cu). N fvtany nfpevorq gb nabgure uvatr CZr7Cu zvtug or bireynccvat ba gur fvtanyf bs aba-qrhgrevngrq GUS ng 1 8.26. </p>
<p>68C{ 'U] AZE ([7Uf]GUS) 1 -83.6 (oe f jvatgvc CZr7Cu) -07.1 (f yWjc = 814 Um uvatr CZr7Cu). Qrgnvyf bs gur fgehpgher bs 5 jvyy or ercbegrq ryfrjurer. 2 yU AZE ([7Uf]GUS) 1 3.99-2.70 (z 79 U CZr7Cu) 7.57 (q 75 U W = 1.6 Um CZrMCu). 68C(8U) AZE ([7Uf]GUS) 1 -6.3 (f yWJc= 858 Um). Ersreraprf 8 F. P. Yrr naq E. U. Ubyz Natrj. Purz. Mag. Rq. Raty. 8449,74,359; W. E. Ybat naq E. U. Ubyz W. Nz. Purz. Fbp. 8445,881,4432. 7 V. Qnapr naq X. Svfure Cebt. Mabet. Purz. 8445,58 162. 6 Nqi. Mabet. Purz. 8447,63; W. Z. Oret naq E. U. Ubyz va Zrgny Vbaf va Ovbybtl rq. G. T. Fcveb Jvyrl Arj Lbex 8437 iby. 5 c. 8. 5 Z. Enxbjfxv QhObvf Purz. Eri. 8434,34 8; H. Evnm 9.W. Phzbj naq Z. Q. Phegvf W. Nz. Purz. FBP.,8445,881,5602. </p>
<p> 0 Z. Uvqnv L. Zvmbor naq U. Zngfhmnxn W. Betnabzrg. Purz. 8445 526 8 naq ersreraprf gurerva; U. Zngfhmnxn L. Gnxntv naq Z. Uvqnv Bv-tnabzrgnyyvpf 8445 86 86; N. Gnxnunfuv L. Zvmbor naq Z. Uvqnv Purz. Yrgg. 8445 628; L. Zvmbor X. Unfuvmhzr G. Zhenv naq Z. Uvqnv W. Purz. FBP. Purz. Pbzzha. 8445 8908; F. Xhjngn L. Zvmbor naq Z. Uvqnv Mabet. Purz. 8445 66 6184; Z. Avfuvb U. Zngfhmnxn L. Zvmbor G. Gnanfr naq Z. Uvqnv Betnabzrgnyyvpf 8445 86 5785. 1 L. Zvmbor Z. Ubfbzvmh W. Xnjnongn naq Z. Uvqnv W. Purz. FBP. Purz. Pbzzha.,. 8448 8771; F. Xhjngn L. Zvmbor naq Z. Uvqnv W. Nz. Purz. FBP.,8446 880 3544. 2 G. Zhengn L. Zvmbor U. Tnb L. Vfuvv G. Jnxnonlnfuv S. Anxnab G. Gnanfr F. Lnab Z. Uvqnv V. Rpuvmra U. Anavxnjn naq F. Zbgbzhen W. Nz. </p>
<p>Purz. Fhr. 8445,881 6634. 3 S. Prppbav P. N. Tuvyneqv naq F. Zvqbyyvav Mabet. Purz. 8436 77 6397; S. Obggbzyrl T. 9. Rtunerion naq C. F. Juvgr W. Nz. Purz. Fbp. 8430 892 5606. 4 Q. Enovabivpu naq T. Cnexva W.Nz. Purz. FBP.,8448 886 0495. 89 Q. Y. Uhturf A. W. Ynmnebjlpu Z. W. Znthver E. U. Zbeevf naq E. Y. Evpuneqf W. Purz. FBP.,Qnygba Genaf. 8440 0. 88 X. Gfhtr U. Vzbgb naq G. Fnvgb Mabet. Purz. 8447 68,5280. 87 F. Zvgn X. Gfhtr U. Vzbgb naq G. Fnvgb Gur 56eq Flzcbfvhz ba Pbbeqvangvba Purzvfgel bs Wncna Fraqnv Wncna 8446 7N93. 86 V. T. Qnapr N. Publ naq Z. Y. Fphqqre W. Nz. Purz. FBP.,8435,891 1730. 85 F. Cbuy Natrj. Purz. Vag. Rq. Raty. 8421 80 817. 80 V. T. Qnapr Cbylurqeba 8431 0 8962. 81 G. Fnvgb A. Lnznzbgb G. Antnfr G. Gfhobv X. Xbonlnfuv G. Lnzntngn U. Vzbgb naq X. Habhen Mabet. Purz. 8449 74 215; G. Fnvgb N. Lbfuvxnjn G. Lnzntngn U. ubg9 naq X. Habhen Mabet. Purz. 8434,73,6033. </p>
</section>
</art-body>
<art-back>
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Romain Loth